Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Methoxybenzaldehyde → 6-bromo-2-(2-methoxyphenyl)-N-(2,4,4-trimethylpentan-2-yl)imidazo[1,2-a]pyridin-3-amine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Methoxybenzaldehyde | HCID 8658 | — |
| 반응물 | 1,1,3,3-Tetramethylbutyl isocyanide | HCID 26725 | — |
| 반응물 | 2-Amino-5-bromopyridine | HCID 70622 | — |
| 용매 | Perchloric Acid | HCID 24247 | — |
| 생성물 | 6-bromo-2-(2-methoxyphenyl)-N-(2,4,4-trimethylpentan-2-yl)imidazo[1,2-a]pyridin-3-amine | HCID 3532132 | — |
반응 단계
Compound (13) was prepared according to the general synthesis instructions from 1.0 ml of 2-amino-5-bromopyridine solution (0.1 M, DCM), 0.575 ml of 1,1,3,3-tetramethylbutyl isocyanide solution (0.2 M, DCM), 0.500 ml of 2-methoxybenzaldehyde solution (0.3 M, DCM), and 10 μl of perchloric acid (w=20%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06849642B2 |
| 출처 데이터셋 | uspto-grants-2005_02 |
| ORD ID | ord-fd9e70201c864437b2080fdccf512e23 |
| 출처 메모 | uspto-grants-2005_02 |