Diethylamine → N-[2-(Diethylamino)ethyl]undecanamide

HRID 2286008

반응식

HRID 2286008 반응식
[CH2:1]([C:12]1[O:13][CH2:14][CH2:15][N:16]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10]C.[CH2:17]([NH:19][CH2:20][CH3:21])[CH3:18]>C([O-])(=O)C.[Zn+2].C([O-])(=O)C>[CH2:17]([N:19]([CH2:20][CH3:21])[CH2:14][CH2:15][NH:16][C:12](=[O:13])[CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10])[CH3:18]

참가 물질

4

반응물 2

HCID 8021DiethylamineHCID 3470762-Undecyl-2-oxazoline

생성물 1

HCID 13632622N-[2-(Diethylamino)ethyl]undecanamide수율 87%

시약·촉매·용매 1

HCID 11192Zinc Acetate촉매

실험 절차

Undecyloxazoline (53 mmoles), diethylamine (104 mmoles) and 0.9 mmole of zinc acetate are reacted under conditions similar to Example 2 to yield 87 percent of theoretical N-(2-diethylaminoethyl)undecylamide.

출처 및 근거

ORD 기록
ord-18e5565f4cd9498e9f10f8808ad9ab5e
출처 데이터셋
uspto-grants-1982_04
특허 번호
US04326067

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