Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3,5-Dimethylcyclohex-2-en-1-one → 1,3-Dimethyl-5-oxocyclohexanephosphonic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3,5-Dimethylcyclohex-2-en-1-one | HCID 14291 | — |
| 반응물 | Diethylphosphite | HCID 3780918 | — |
| 용매 | Hydrochloric Acid | HCID 313 | — |
| 생성물 | 1,3-Dimethyl-5-oxocyclohexanephosphonic acid | HCID 23462674 | — |
| 생성물 | Diethyl 1,3-dimethyl-5-oxocyclohexanephosphonate | HCID 23462678 | — |
반응 단계
Diethyl 1,3-dimethyl-5-oxocyclohexanephosphonate (B. pt. 120°/0.1 mm) was prepared by the base catalysed addition of diethylphosphite to 3,5-dimethyl-2-cyclohexen-1-one. Hydrolysis of the ester in concentrated HCl gave 1,3-dimethyl-5-oxocyclohexanephosphonic acid as a viscous oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04265769 |
| 출처 데이터셋 | uspto-grants-1981_05 |
| ORD ID | ord-069ca0d613fc4c73b63845d4b9818048 |
| 출처 메모 | uspto-grants-1981_05 |