Urea → Tetrakis(ureidomethyl)phosphonium chloride

HRID 2286380노트

반응식

HRID 2286380 반응식
[CH2:1]([P+:3]([CH2:8]O)([CH2:6]O)[CH2:4]O)O.[Cl-:10].[NH2:11][C:12]([NH2:14])=[O:13]>>[Cl-:10].[NH:11]([CH2:8][P+:3]([CH2:1][NH:11][C:12]([NH2:14])=[O:13])([CH2:4][NH:11][C:12]([NH2:14])=[O:13])[CH2:6][NH:11][C:12]([NH2:14])=[O:13])[C:12]([NH2:14])=[O:13]

참가 물질

3

반응물 2

HCID 1176UreaHCID 31298Tetrakis(hydroxymethyl)phosphonium chloride

생성물 1

HCID 23463266Tetrakis(ureidomethyl)phosphonium chloride수율 100.9%

실험 절차

Reaction of 80% THPC (23.82 g, 0.1 mol) with urea (24.02 g, 0.4 mol), following Example 3, gave 36.18 g (100.8%) of tetrakis(ureidomethyl)phosphonium chloride (I, R=R'=R"=H, X=Cl) as a colorless, brittle glass, identical (31P NMR) to the product of Example 11.

출처 및 근거

ORD 기록
ord-15ea4bcac9384411bb9a9dade0ebb434
출처 데이터셋
uspto-grants-1981_05
특허 번호
US04265945

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