Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Triethyl phosphite → Diethyl (3,3-diphenylallyl)phosphonate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Triethyl phosphite | HCID 31215 | — |
| 반응물 | 3-Chloro-1,1-diphenylpropene | HCID 12890165 | — |
| 생성물 | Diethyl (3,3-diphenylallyl)phosphonate | HCID 13328742 | 108.2% |
반응 단계
A mixture of 40.8 g (0.155 mol) of 3,3-diphenylallyl chloride (11a) and 94.48 g (0.569 mol) of triethyl phosphite was stirred with refluxing for 24 hours. The disappearance of the 3,3-diphenylallyl chloride (11a) was ascertained, before the reaction was terminated. After cooling, the reaction mixture was distilled with a Claisen flask equipped with a vigreux to obtain 55.39 g of the target compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06083651 |
| 출처 데이터셋 | uspto-grants-2000_07 |
| ORD ID | ord-d7ec43e8937e4924a5069c81784bbde9 |
| 출처 메모 | uspto-grants-2000_07 |