Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Oxalyl chloride → 2,3-Dichloro-6-iodobenzoic acid chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Oxalyl chloride | HCID 65578 | — |
| 반응물 | 2,3-Dichloro-6-iodobenzoic acid | HCID 22008816 | — |
| 촉매 | Dimethylformamide | HCID 6228 | — |
| 용매 | Ethyl Acetate | HCID 8857 | — |
| 생성물 | 2,3-Dichloro-6-iodobenzoic acid chloride | HCID 54292031 | — |
반응 단계
DMF (one drop) was added to a stirred solution of 2,3-dichloro-6-iodobenzoic acid (1.53 g, 4.83 mmol) and oxalyl chloride (2 ml) in ethyl acetate (20 ml). After 2 hours, the solution was evaporated and the product was used immediately.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06083952 |
| 출처 데이터셋 | uspto-grants-2000_07 |
| ORD ID | ord-fcb6181488fb4a4085cac970464cc3d3 |
| 출처 메모 | uspto-grants-2000_07 |