Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
(4,5-Dimethylfuran-2-yl)-(4,5-dimethylthiazol-2-yl)methanol → (4,5-Dimethylfuran-2-yl)(4,5-dimethylthiazol-2-yl)-methanone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | (4,5-Dimethylfuran-2-yl)-(4,5-dimethylthiazol-2-yl)methanol | HCID 23078354 | — |
| 촉매 | HCID 178418406 | HCID 178418406 | — |
| 용매 | Chloroform | HCID 6212 | — |
| 생성물 | (4,5-Dimethylfuran-2-yl)(4,5-dimethylthiazol-2-yl)-methanone | HCID 23078247 | 97.1% |
반응 단계
(4,5-Dimethylfuran-2-yl)-(4,5-dimethylthiazol-2-yl)methanol (945 mg) was dissolved in chloroform (20 ml) to prepare a solution. Manganese dioxide (3.5 g) was added to the solution, and the mixture was stirred at room temperature overnight. The reaction solution was filtered through Celite, and the solvent was removed from the filtrate by distillation under the reduced pressure to give (4,5-dimethylfuran-2-yl)(4,5-dimethylthiazol-2-yl)-methanone (910 mg, yield 97%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07560558B2 |
| 출처 데이터셋 | uspto-grants-2009_07 |
| ORD ID | ord-ff9c0126c13c495080a3055c9946dee9 |
| 출처 메모 | uspto-grants-2009_07 |