Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Pyrimidine → HCID 54493243, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Pyrimidine | HCID 9260 | — |
| 반응물 | Methanesulfonyl chloride | HCID 31297 | — |
| 반응물 | (S)-(+)-3-Methyl-1-pentanol | HCID 641003 | — |
| 생성물 | HCID 54493243 | HCID 54493243 | 46.42% |
반응 단계
In a flask were charged 15.89 g of (S)-3-methylpentanol and 65 ml of pyrimidine. After cooling to 0° to 50° C., 23.63 g of methanesulfonyl chloride was added thereto dropwise, and the mixture was allowed to react at the same temperature for 1 hour. The reaction mixture was extracted with diethyl ether, and the extract was washed with water and concentrated to obtain 12.14 g (46.42%) of the titled compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06093345 |
| 출처 데이터셋 | uspto-grants-2000_07 |
| ORD ID | ord-5da116c9920b45c5b94894bd56232f10 |
| 출처 메모 | uspto-grants-2000_07 |