Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Itaconic acid → 5-Oxo-1-(3-{(benzylamino)carbonylamino}-5-(trifluoromethyl)phenyl)pyrrolidine-3-carboxylic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Itaconic acid | HCID 811 | — |
| 반응물 | n-(3-Amino-5-(trifluoromethyl)phenyl)(benzylamino)carboxamide | HCID 22591859 | — |
| 생성물 | 5-Oxo-1-(3-{(benzylamino)carbonylamino}-5-(trifluoromethyl)phenyl)pyrrolidine-3-carboxylic acid | HCID 22591872 | — |
반응 단계
A mixture of N-(3-amino-5-(trifluoromethyl)phenyl)(benzylamino)carboxamide and itaconic acid was fused at 110° C. for 10 hours. The resulted solid was washed with methanol and then dried at 50° C. for 12 hours.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06849639B2 |
| 출처 데이터셋 | uspto-grants-2005_02 |
| ORD ID | ord-864cef6e6f664a059be8b4a512c33fb1 |
| 출처 메모 | uspto-grants-2005_02 |