참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | Cyanuric chloride | HCID 7954 | — |
| 반응물 | Dodecyl 4-aminobenzoate | HCID 328885 | — |
| 용매 | O-Xylene | HCID 7237 | — |
| 생성물 | 1,3,5-Tris-(p-(dodec-1-yloxycarbonyl)-anilino)-s-triazine | HCID 20152739 | — |
반응 단계
18.5 g of cyanuric chloride and 92 g of dodecyl p-aminobenzoate in 1,000 ml of xylene were heated at 140° C. until HCl gas was no longer evolved. After 8 hours, the reaction solution was cooled to 80° C., washed twice with saturated sodium bicarbonate solution and once with water, and then cooled to room temperature. The precipitated crystals were filtered off under suction and dried.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04617390 |
|---|
| 출처 데이터셋 | uspto-grants-1986_10 |
|---|
| ORD ID | ord-b3521faf55594a34a1d0687365b46fe4 |
|---|
| 출처 메모 | uspto-grants-1986_10 |
|---|
