Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Chloroaniline → 8-Chloro-2-methylquinoline
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Chloroaniline | HCID 7240 | — |
| 반응물 | Crotonaldehyde | HCID 447466 | — |
| 생성물 | 8-Chloro-2-methylquinoline | HCID 221113 | 57% |
반응 단계
The procedure described in Example 1 was followed, except that 130 g/hour of 2-chloroaniline and 84 g/hour of crotonaldehyde were employed. Distillation from the oil bed under 5 mbar until the bottom temperature reached 250° C., and crystallization of the distillate with xylene, gave 101 g (57% of theory) of 8-chloro-2-methylquinoline of melting point 64° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04617395 |
| 출처 데이터셋 | uspto-grants-1986_10 |
| ORD ID | ord-da50df8f3f3f4fb78c0fb85de7b18430 |
| 출처 메모 | uspto-grants-1986_10 |