Methyl behenate → Potassium Behenate

HRID 2291517

반응식

HRID 2291517 반응식
[C:1]([O:24]C)(=[O:23])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22].[OH-].[K+:27]>CO>[C:1]([O-:24])(=[O:23])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22].[K+:27]

참가 물질

4

반응물 2

HCID 13584Methyl behenateHCID 14797Potassium Hydroxide

생성물 1

HCID 23663647Potassium Behenate

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

Methyl behenate (0.375 moles/mole of sucrose to be used in Step B) is saponified by stirring at reflux in methanol containing an equivalent amount of KOH. The reaction is stirred with heating until all methyl ester has been converted to soap as indicated by infrared analysis. The soap solution is used, as is in the next reaction step.

후처리

  1. stirringThe reaction is stirred
  2. customas is in the next reaction step

출처 및 근거

ORD 기록
ord-0df2f8c266604a0898097b9e85e2ee78
출처 데이터셋
uspto-grants-1989_01
특허 번호
US04797300

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