Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Exifone → HCID 14010408, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Exifone | HCID 40399 | — |
| 반응물 | Pivaloyl chloride | HCID 62493 | — |
| 용매 | Pyridine | HCID 1049 | — |
| 생성물 | HCID 14010408 | HCID 14010408 | — |
반응 단계
100 mg of 3,4,5,4',5',6'-hexahydroxy benzophenone (0.00036 mole) and 450 MG (0.004 mole) of pivaloyl chloride were warmed to 50° C. in 20 mls of pyridine for 4 hrs. Solvent removed via N2 stream. Water added and extraction of product was done via CH2Cl2. The organic layer was washed with K2CO3 (5%) and dried over MgSo4. Solvent removal left an oil. 250 mg. (88%) yield.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04801610 |
| 출처 데이터셋 | uspto-grants-1989_01 |
| ORD ID | ord-8d2c2458b1184cd184c7b5162797bcff |
| 출처 메모 | uspto-grants-1989_01 |