Heptanal → HCID 21477974, 화합물

HRID 2292409노트

반응식

C([Li])CCC.[CH:6](=[O:13])[CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12].[F:14][C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][C:16]=1[F:21]>>[F:14][C:15]1[C:16]([F:21])=[CH:17][CH:18]=[CH:19][C:20]=1[CH:6]([OH:13])[CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12]

참가 물질

반응물 3

HCID 8130Heptanal

HCID 97061,2-Difluorobenzene

HCID 178418339Butyllithium

생성물 1

HCID 21477974HCID 21477974, 화합물

실험 절차

Quantities: n-butyllithium (50 cm3, 10.0M in hexanes, 0.5 mol), heptanal (57 g, 0.5 mol) and 1,2-difluorobenzene (57 g, 0.5 mol). The experimental procedure was as described in Example 16.

출처 및 근거

ORD 기록: ord-8a851d4ec5ca4aae8671e365f8157cc0
출처 데이터셋: uspto-grants-1997_11
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US05683623

반응 노트

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