1H-Indene-1-carboxylic acid, 2,3-dihydro- → HCID 18918726, 화합물

HRID 2292647노트

반응식

HRID 2292647 반응식
[CH:1]1([C:10](O)=O)[C:9]2[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=2)[CH2:3][CH2:2]1.[CH3:13][O:14][C:15]1[C:16]([N:24]2[CH2:29][CH2:28][NH:27][CH2:26][CH2:25]2)=[CH:17][C:18]2[O:22][CH2:21][CH2:20][C:19]=2[CH:23]=1.C([O-])(=O)/C=C/C([O-])=O>>[CH3:13][O:14][C:15]1[C:16]([N:24]2[CH2:25][CH2:26][N:27]([CH2:10][CH:1]3[C:9]4[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=4)[CH2:3][CH2:2]3)[CH2:28][CH2:29]2)=[CH:17][C:18]2[O:22][CH2:21][CH2:20][C:19]=2[CH:23]=1

참가 물질

4

반응물 3

HCID 857281H-Indene-1-carboxylic acid, 2,3-dihydro-HCID 5460307FumarateHCID 15839404HCID 15839404, 화합물

생성물 1

HCID 18918726HCID 18918726, 화합물

실험 절차

Prepared as described in Example 9, starting from indan-1-ylcarboxylic acid and 4-(2,3-dihydro-5-methoxybenzofuran-6-yl)piperazine. The fumarate of the title compound melts at 195°-197° C. (ethanol).

후처리

  1. customPrepared

출처 및 근거

ORD 기록
ord-bfdb7a1a99be491bb5583db100ad5090
출처 데이터셋
uspto-grants-1997_11
특허 번호
US05684020

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