4-Chloro-3-nitrobenzoic acid → 4-(allylamino)-3-nitrobenzoic acid

HRID 2292992노트

반응식

HRID 2292992 반응식
[N+:1]([C:4]1[CH:5]=[C:6](N)[CH:7]=[CH:8][C:9]=1[NH:10][CH2:11][CH:12]=[CH2:13])([O-:3])=[O:2].ClC1C=CC([C:20]([OH:22])=[O:21])=CC=1[N+]([O-])=O>>[N+:1]([C:4]1[CH:5]=[C:6]([CH:7]=[CH:8][C:9]=1[NH:10][CH2:11][CH:12]=[CH2:13])[C:20]([OH:22])=[O:21])([O-:3])=[O:2]

참가 물질

3

반응물 2

HCID 73204-Chloro-3-nitrobenzoic acidHCID 23500036N-(2-Nitro-4-aminophenyl)-allylamine

생성물 1

HCID 117155314-(allylamino)-3-nitrobenzoic acid

실험 절차

Synthesis and working up as for compound 1, but with 4-chloro-3-nitrobenzoic acid instead of 4-fluoro-3-nitroaminobenzene. Yellow crystals, melting point 195°-200° C.

후처리

  1. customSynthesis

출처 및 근거

ORD 기록
ord-aa1f2bcaee274f7ea292346926f4c329
출처 데이터셋
uspto-grants-1997_11
특허 번호
US05685881

반응 노트

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