Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Phosgene → Tetradecyl chloroformate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Phosgene | HCID 6371 | — |
| 반응물 | 1-Tetradecanol | HCID 8209 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | Tetradecyl chloroformate | HCID 92493 | 98.7% |
반응 단계
29 ml of a 20% toluene solution of phosgene (55.98 mmoles) was added to tetradecyl alcohol (4 g, 18.66 mmoles) and the reaction mixture was left to stand for 20 hours under stirring at room temperature. After solvent evaporation, the residue was taken up with hexane and evaporated to dryness (several times) to give 5.1 g product as colourless liquid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | USRE040861E1 |
| 출처 데이터셋 | uspto-grants-2009_07 |
| ORD ID | ord-2d13dd51f1cf434baf640ddf914ee0aa |
| 출처 메모 | uspto-grants-2009_07 |