Tetrahydrofuran → HCID 21476517, 화합물
반응식
[H-].[Al+3].[Li+].[H-].[H-].[H-].O1CCCC1.C([O:14][C:15]([CH2:17][NH:18][CH:19]([C:21]1[CH:26]=[CH:25][CH:24]=[CH:23][C:22]=1[CH3:27])[CH3:20])=O)C>O>[OH:14][CH2:15][CH2:17][NH:18][CH:19]([C:21]1[CH:26]=[CH:25][CH:24]=[CH:23][C:22]=1[CH3:27])[CH3:20]참가 물질
5
실험 절차
To a mixture of 3.8 g of lithium aluminium hydride (0.1M) and 150 ml of tetrahydrofuran, 23.3 g of the compound (0.105M) prepared in Step 2 above was dropwise added at room temperature and stirred for 30 minutes. The resultant was added with water and solids produced were filtered. The filtrate was dried over anhydrous sodium sulfate and concentrated under a reduced pressure, to give 13.8 g of the title compound.
후처리
- additionabove was dropwise added at room temperature
- customproduced
- filtrationwere filtered
- dry with materialThe filtrate was dried over anhydrous sodium sulfate
- concentrationconcentrated under a reduced pressure
출처 및 근거
- ORD 기록
- ord-d27c09a32e4e4329baf030e0a5a47bc3
- 출처 데이터셋
- uspto-grants-1997_11
- 특허 번호
- US05686458
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