Morpholine → HCID 66738942, 화합물

HRID 229331노트

반응식

HRID 229331 반응식
[C:1](#[N:10])[CH:2]=[CH:3][C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1.[CH3:11][C:12]1[NH:16][N:15]=[C:14]([NH2:17])[CH:13]=1.[NH:18]1[CH2:23][CH2:22][O:21][CH2:20][CH2:19]1>>[CH3:11][C:12]1[NH:16][N:15]=[C:14]([NH:17][C:3]2[CH:2]=[C:1]([N:18]3[CH2:23][CH2:22][O:21][CH2:20][CH2:19]3)[N:10]=[C:1]([CH:2]=[CH:3][C:4]3[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=3)[N:10]=2)[CH:13]=1

참가 물질

4

반응물 3

HCID 8083MorpholineHCID 746673-Phenylprop-2-enenitrileHCID 931461H-Pyrazol-3-amine, 5-methyl-

생성물 1

HCID 66738942HCID 66738942, 화합물

실험 절차

Example 64 was synthesized via Scheme 6 according to the general scheme provided above with the appropriate starting materials cinnamonitrile, 5-methyl-1H-pyrazole-3-amine, and morpholine. Structure of the target was confirmed by 1H-NMR. The 1H-NMR is attached.

후처리

  1. customExample 64 was synthesized via Scheme 6 according to the general scheme
  2. customprovided above with the

출처 및 근거

ORD 기록
ord-fb63ec93abaa45309b099636ab709be4
출처 데이터셋
uspto-grants-2009_07
특허 번호
US07563787B2

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