Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Tridecanal → Tridecanedioic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Tridecanal | HCID 25311 | — |
| 반응물 | Nonanal | HCID 31289 | — |
| 반응물 | Erucic Acid | HCID 5281116 | — |
| 생성물 | Tridecanedioic acid | HCID 10458 | — |
반응 단계
338.58 g (1 mol) of erucic acid (purity 95%) were ozonized in analogy to Example 1 and then hydrogenation was carried out. The hydrogenation solution obtained in this way contained nonanal and tridecanealdehyde acid and was divided by distillation. For oxidation, the corresponding aldehyde fraction was employed and was oxidized at 14 bar in analogy to Example 1. 185 g of tridecanedioic acid per cycle were obtained with a purity of 95%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05686638 |
| 출처 데이터셋 | uspto-grants-1997_11 |
| ORD ID | ord-1c2aa7fad9214de9be3b156d3fed97a7 |
| 출처 메모 | uspto-grants-1997_11 |