Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → 3-Methoxy-4-phenylaminopyrrolidine hydrochloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | 1-t-Butoxycarbonyl-3-methoxy-4-phenylaminopyrrolidine | HCID 21473342 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | 3-Methoxy-4-phenylaminopyrrolidine hydrochloride | HCID 21473354 | — |
반응 단계
In 100 ml of methanol was dissolved 1.98 g (0.0068 mole) of 1-t-butoxycarbonyl-3-methoxy-4-phenylaminopyrrolidine obtained as described above, and 23.5 ml of 6N hydrochloric acid was added thereto. The mixture was left to stand at room temperature overnight. The solvent was removed under reduced pressure, and the residue was washed with ethanol to obtain 1.71 g of 3-methoxy-4-phenylaminopyrrolidine hydrochloride as white powder.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05688791 |
| 출처 데이터셋 | uspto-grants-1997_11 |
| ORD ID | ord-0cc71dc497264b3cb7f2d3b3eb386623 |
| 출처 메모 | uspto-grants-1997_11 |