Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Dimethylaminopyridine → HCID 178469736, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Dimethylaminopyridine | HCID 21885 | — |
| 반응물 | Ethyl 4-chloro-2-phenylpyrimidine-5-carboxylate | HCID 239537 | — |
| 반응물 | HCID 178419079 | HCID 178419079 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | HCID 178469736 | HCID 178469736 | — |
반응 단계
Ethyl 4-chloro-2-phenyl-5-pyrimidinecarboxylate and N-tert-butoxycarbonyl-trans-1,4-cyclohexanediamine were reacted in ethanol in the presence of dimethylaminopyridine in the same manner as in Reference Example 3-49 to obtain N-tert-butoxycarbonyl-trans-4-(5-ethoxycarbonyl-2-phenyl-4-pyrimidinylamino)cyclohexylamine.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06849622B2 |
| 출처 데이터셋 | uspto-grants-2005_02 |
| ORD ID | ord-9e5d3733bff0495f939a8e37a575b5e3 |
| 출처 메모 | uspto-grants-2005_02 |