참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 2,4-Dinitroiodobenzene | HCID 69730 | — |
| 반응물 | Diethyl 5-tributylstannyl-2-furanphosphonate | HCID 22280515 | — |
| 촉매 | Tetrakis(triphenylphosphine)palladium | HCID 11979704 | — |
| 용매 | 1,4-Dioxane | HCID 31275 | — |
| 생성물 | Diethyl 5-(3,5-dinitrophenyl)-2-furanphosphonate | HCID 22349210 | — |
반응 단계
A mixture of diethyl 5-tributylstannyl-2-furanphosphonate (1 mmol), 1-iodo-2,4-dinitrobenzene (1 mmol) and tetrakis(triphenylphosphine)-palladium(0) (0.05 mmol) in 6 mL of dioxane was heated at 80° C. for 16 h. Evaporation of solvent and chromatography provided diethyl 5-(3,5-dinitrophenyl)-2-furanphosphonate as solid foam.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US07563774B2 |
|---|
| 출처 데이터셋 | uspto-grants-2009_07 |
|---|
| ORD ID | ord-9ba19b201669434ead85defe26c61962 |
|---|
| 출처 메모 | uspto-grants-2009_07 |
|---|
