3-Tert-butyl-4-methoxybenzoyl chloride → HCID 21474569, 화합물

HRID 2294585노트

반응식

HRID 2294585 반응식
[C:1]([C:5]1[CH:6]=[C:7]([CH:11]=[CH:12][C:13]=1[O:14][CH3:15])[C:8](Cl)=[O:9])([CH3:4])([CH3:3])[CH3:2].[OH:16][CH2:17][C:18]1[S:22][C:21]([C:23]([O:25][CH2:26][CH:27]=[CH2:28])=[O:24])=[CH:20][CH:19]=1>>[C:1]([C:5]1[CH:6]=[C:7]([CH:11]=[CH:12][C:13]=1[O:14][CH3:15])[C:8]([O:16][CH2:17][C:18]1[S:22][C:21]([C:23]([O:25][CH2:26][CH:27]=[CH2:28])=[O:24])=[CH:20][CH:19]=1)=[O:9])([CH3:4])([CH3:3])[CH3:2]

참가 물질

3

반응물 2

HCID 136335553-Tert-butyl-4-methoxybenzoyl chlorideHCID 21474497HCID 21474497, 화합물

생성물 1

HCID 21474569HCID 21474569, 화합물

실험 절차

In a manner similar to Example 1(d), by reaction of 1.6 g (7 mmol) of 3-tert-butyl-4-methoxybenzoyl chloride with 1.4 g (7 mmol) of allyl 5-hydroxymethyl-2-thiophenecarboxylate, 1.5 g (55%) of allyl ester are obtained in the form of a slightly yellow oil.

후처리

  1. customare obtained in the form of a slightly yellow oil

출처 및 근거

ORD 기록
ord-d0e1561c737240ac8d97c6818757ad43
출처 데이터셋
uspto-grants-1997_11
특허 번호
US05688817

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