3-Tert-butyl-4-methoxybenzoyl chloride → Allyl 2-hydroxy-4-(3-tert-butyl-4-methoxybenzoyloxymethyl)benzoate

HRID 2294589

반응식

HRID 2294589 반응식
[C:1]([C:5]1[CH:6]=[C:7]([CH:11]=[CH:12][C:13]=1[O:14][CH3:15])[C:8](Cl)=[O:9])([CH3:4])([CH3:3])[CH3:2].[OH:16][CH2:17][C:18]1[CH:29]=[CH:28][C:21]([C:22]([O:24][CH2:25][CH:26]=[CH2:27])=[O:23])=[C:20]([OH:30])[CH:19]=1>>[OH:30][C:20]1[CH:19]=[C:18]([CH2:17][O:16][C:8](=[O:9])[C:7]2[CH:11]=[CH:12][C:13]([O:14][CH3:15])=[C:5]([C:1]([CH3:3])([CH3:2])[CH3:4])[CH:6]=2)[CH:29]=[CH:28][C:21]=1[C:22]([O:24][CH2:25][CH:26]=[CH2:27])=[O:23]

참가 물질

3

반응물 2

HCID 136335553-Tert-butyl-4-methoxybenzoyl chlorideHCID 21474558Allyl 4-hydroxymethyl-2-hydroxybenzoate

생성물 1

HCID 21474526Allyl 2-hydroxy-4-(3-tert-butyl-4-methoxybenzoyloxymethyl)benzoate

실험 절차

In a manner similar to Example 1(d), by reaction of 2.4 g (10.5 mmol) of 3-tert-butyl-4-methoxybenzoyl chloride with 2.2 g (10.5 mmol) of allyl 4-hydroxymethyl-2-hydroxybenzoate, 2.5 g (61%) of the expected allyl ester are obtained in the form of a slightly yellow oil.

후처리

  1. customare obtained in the form of a slightly yellow oil

출처 및 근거

ORD 기록
ord-3fd2230ffb6d4043807846fb672aac58
출처 데이터셋
uspto-grants-1997_11
특허 번호
US05688817

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