Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ammonia → Aklomide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ammonia | HCID 222 | — |
| 반응물 | Benzoyl chloride, 2-chloro-4-nitro- | HCID 81522 | — |
| 생성물 | Aklomide | HCID 2075 | 90% |
반응 단계
Thereafter, 2-chloro-4-nitrobenzoyl chloride (450 g, 2.1 m) was added dropwise to a stirred 28% ammonia solution (2,000 ml) at below room temperature between 9° and 16° C. The precipitated reaction mixture was washed with water and 30% methanol and then vacuum-dried to yield 2-chloro-4-nitrobenzamide (379 g, 90%, mp 168°-170° C.).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04424371 |
| 출처 데이터셋 | uspto-grants-1984_01 |
| ORD ID | ord-9cec857d21fd40069e2cb33d97c7ca65 |
| 출처 메모 | uspto-grants-1984_01 |