Ammonia → α-Phenyl-2-benzothiazolemethanamine

HRID 2295486노트

반응식

HRID 2295486 반응식
Cl.[NH2:2][CH:3]([C:10]1[S:11][C:12]2[CH:18]=[CH:17][CH:16]=[CH:15][C:13]=2[N:14]=1)[C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1.N>C(Cl)Cl>[NH2:2][CH:3]([C:10]1[S:11][C:12]2[CH:18]=[CH:17][CH:16]=[CH:15][C:13]=2[N:14]=1)[C:4]1[CH:5]=[CH:6][CH:7]=[CH:8][CH:9]=1

참가 물질

4

반응물 2

HCID 222AmmoniaHCID 23318519HCID 23318519, 화합물

생성물 1

HCID 13342005α-Phenyl-2-benzothiazolemethanamine

시약·촉매·용매 1

HCID 6344Dichloromethane용매

실험 절차

The hydrochloride was dissolved with aqueous ammonia and methylene chloride, the aqueous layer was extracted with two portions of methylene chloride. The combined methylene chloride extracts were washed with brine, dried over Na2SO4, filtered and concentrated in vacuo. 13.1 g. of white solid of desired producted was obtained, mp. 68°-70° C.

후처리

  1. extractionthe aqueous layer was extracted with two portions of methylene chloride
  2. washThe combined methylene chloride extracts were washed with brine
  3. dry with materialdried over Na2SO4
  4. filtrationfiltered
  5. concentrationconcentrated in vacuo
  6. customof white solid of desired producted was obtained

출처 및 근거

ORD 기록
ord-437c62e85e7d49d09e9685a0b2096388
출처 데이터셋
uspto-grants-1984_01
특허 번호
US04425338

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