Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Trifluoromethanesulfonic acid → Trifluoromethanesulfonic acid--1-ethyl-1H-imidazole (1/1)
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Trifluoromethanesulfonic acid | HCID 62406 | — |
| 반응물 | 1-Ethyl-1H-imidazole | HCID 81540 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | Trifluoromethanesulfonic acid--1-ethyl-1H-imidazole (1/1) | HCID 71366743 | — |
반응 단계
Twenty-five grams of trifluoromethanesulfonic acid was added dropwise to a solution of 16 g of N-ethylimidazole in 20 ml of ethanol at 0° C. The solution was returned to room temperature, stirred overnight, and dried in vacuo at 60° C. for 16 hours to give N-ethylimidazole trifluoromethanesulfonate (EtIm+TfS−) as a colorless transparent liquid. The resulting salt had a melting point of 8.3° C. (literature value: 7.8° C.).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07563850B2 |
| 출처 데이터셋 | uspto-grants-2009_07 |
| ORD ID | ord-3f8aa552171f467c91de8f7246dc2cc5 |
| 출처 메모 | uspto-grants-2009_07 |