Ethyl ketone → HCID 54559161, 화합물

HRID 2295704노트

반응식

HRID 2295704 반응식
Cl[CH2:2][CH:3]=[C:4]([CH3:7])[CH:5]=[CH2:6].[CH3:8][CH2:9][C:10](=[O:13])[CH2:11][CH3:12].[OH-].[K+]>CCCCC>[CH3:8][CH:9]([CH2:6][CH:5]=[C:4]([CH3:7])[CH:3]=[CH2:2])[C:10](=[O:13])[CH2:11][CH3:12]

참가 물질

5

반응물 3

HCID 7288Ethyl ketoneHCID 14797Potassium HydroxideHCID 537271125-Chloro-3-methylpenta-1,3-diene

생성물 1

HCID 54559161HCID 54559161, 화합물수율 61.7%

시약·촉매·용매 1

HCID 8003Pentane용매

실험 절차

According to the procedure described in Example 1, from 58 g of 1-chloro-3-methyl-2,4-pentadiene and 43 g of pentan-3-one (diethyl ketone) in the presence of 50 g of powdered potassium hydroxide in 200 ml of dry pentane there are obtained 51 g of crude 4,7-dimethyl-6,8-nonadien-3-one which are subjected to a fractional distillation.

출처 및 근거

ORD 기록
ord-0f0dcf303a26475f9b711546ed719039
출처 데이터셋
uspto-grants-1984_01
특허 번호
US04426321

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