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Ethanol → 5'-Amino-1'-phenyl-[2,3'-bipyridin]-6'(1'H)-one

HRID 229649
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인쇄 미리보기

반응식

HRID 229649 반응식
C(O)C.[N+:4]([C:7]1[C:8](=[O:25])[N:9]([C:19]2[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=2)[CH:10]=[C:11]([C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][N:14]=2)[CH:12]=1)([O-])=O>[H][H].[C].[Pd]>[NH2:4][C:7]1[C:8](=[O:25])[N:9]([C:19]2[CH:20]=[CH:21][CH:22]=[CH:23][CH:24]=2)[CH:10]=[C:11]([C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][N:14]=2)[CH:12]=1
참가 물질실험 절차후처리출처 및 근거반응 노트

참가 물질

5

반응물 2

HCID 702EthanolHCID 223189563-Nitro-1-phenyl-5-(2-pyridyl)-1,2-dihydropyridin-2-one

생성물 1

HCID 223191195'-Amino-1'-phenyl-[2,3'-bipyridin]-6'(1'H)-one수율 83.8%

시약·촉매·용매 2

HCID 178418390HCID 178418390, 화합물촉매HCID 178418361HCID 178418361, 화합물용매

실험 절차

100 mg of 10% palladium-carbon was added to 20 ml of an ethanol solution containing 546 mg of 3-nitro-1-phenyl-5-(pyridin-2-yl)-1,2-dihydropyridin-2-one, followed by stirring overnight in hydrogen atmosphere. The reaction mixture was filtered through silica gel and concentrated, to give 411 mg of the title compound.

후처리

  1. filtrationThe reaction mixture was filtered through silica gel
  2. concentrationconcentrated

출처 및 근거

ORD 기록
ord-8097c69d60324cfea34958ef5b74cc03
출처 데이터셋
uspto-grants-2009_07
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US07563811B2

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