Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Ethylcyclohexan-1-amine → 2-Ethylaniline
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Ethylcyclohexan-1-amine | HCID 544854 | — |
| 반응물 | Calciumoxide | HCID 6850728 | — |
| 반응물 | Alumina | HCID 9989226 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 생성물 | 2-Ethylaniline | HCID 11357 | 95% |
반응 단계
The procedure described in Example 27 is followed, using a reaction temperature of 250° C. and a catalyst which contains 0.5% by weight of palladium on a mixture of 19.4% by weight of calcium oxide and 80.6% by weight of aluminum oxide, and starting from 2-ethylcyclohexylamine. o-Ethylaniline (boiling point=210° C.) is obtained in a yield of 95% of the theory.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04429155 |
| 출처 데이터셋 | uspto-grants-1984_01 |
| ORD ID | ord-7047ce36165548e0b0dda930a92fa923 |
| 출처 메모 | uspto-grants-1984_01 |