Oxalyl chloride → HCID 22742433, 화합물

HRID 2296723노트

반응식

HRID 2296723 반응식
[CH3:1][C:2]1[CH:3]=[CH:4][C:5]2[C:6](=O)[C:7]3[C:12]([N:13]([CH2:17][CH2:18][CH2:19][N:20]4[C:24](=[O:25])[C:23]5=[CH:26][CH:27]=[CH:28][CH:29]=[C:22]5[C:21]4=[O:30])[C:14]=2[C:15]=1[CH3:16])=[CH:11][CH:10]=[CH:9][CH:8]=3.C(Cl)(=O)C([Cl:35])=O>ClCCl>[Cl-:35].[CH3:1][C:2]1[CH:3]=[CH:4][C:5]2[C:14]([C:15]=1[CH3:16])=[N+:13]([CH2:17][CH2:18][CH2:19][N:20]1[C:24](=[O:25])[C:23]3=[CH:26][CH:27]=[CH:28][CH:29]=[C:22]3[C:21]1=[O:30])[C:12]1[C:7](=[CH:8][CH:9]=[CH:10][CH:11]=1)[C:6]=2[Cl:35]

참가 물질

4

반응물 2

HCID 65578Oxalyl chlorideHCID 227424473,4-Dimethyl-10-(3-phthalimidopropyl)-9-acridone

생성물 1

HCID 22742433HCID 22742433, 화합물

시약·촉매·용매 1

HCID 6344Dichloromethane용매

실험 절차

A mixture of 1.0 g of 3,4-dimethyl-10-(3-phthalimidopropyl)-9-acridone with 340 ml of oxalyl chloride was stirred at room temperature in 100 ml of dichloromethane for 30 min. After evaporating the excessive oxalyl chloride and dichloromethane under reduced pressure, 1.1 g of the title compound was obtained.

후처리

  1. customAfter evaporating the excessive oxalyl chloride and dichloromethane under reduced pressure

출처 및 근거

ORD 기록
ord-7a3d397720204f41a4d54f1c2934b094
출처 데이터셋
uspto-grants-2002_12
특허 번호
US06489336B2

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