Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzophenone imine → 5-Bromo-N-(diphenylmethylene)-2-thiazolamine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzophenone imine | HCID 136809 | — |
| 반응물 | 5-Bromothiazol-2-amine monohydrobromide | HCID 2723848 | — |
| 용매 | 1,2-Dichloroethane | HCID 11 | — |
| 생성물 | 5-Bromo-N-(diphenylmethylene)-2-thiazolamine | HCID 11221592 | 82.9% |
반응 단계
26 g of benzophenone imine are added to 34 g of 5-bromo-1,3-thiazol-2-amine hydrobromide, in suspension in 300 ml of 1,2-dichloroethane. The mixture is kept under reflux for 18 hours. The precipitate formed is filtered and the filtrate is concentrated to give 37.2 g of solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07563903B2 |
| 출처 데이터셋 | uspto-grants-2009_07 |
| ORD ID | ord-905f5b86eaf74828a0a1af57bd348d0a |
| 출처 메모 | uspto-grants-2009_07 |