Benzyl Isothiocyanate → 2-(4-Benzyl-5-benzylsulfanyl-1,2,4-triazol-3-yl)pyridine

HRID 229763

반응식

[N:1]1[CH:6]=[CH:5][CH:4]=[CH:3][C:2]=1[C:7]([NH:9][NH2:10])=O.[CH2:11]([N:18]=[C:19]=[S:20])[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1.[CH2:21](Br)[C:22]1[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=1>>[CH2:11]([N:18]1[C:19]([S:20][CH2:21][C:22]2[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=2)=[N:10][N:9]=[C:7]1[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][N:1]=1)[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1

참가 물질

반응물 3

HCID 2346Benzyl Isothiocyanate

HCID 7498Benzyl Bromide

HCID 255881Picolinohydrazide

생성물 1

HCID 114624952-(4-Benzyl-5-benzylsulfanyl-1,2,4-triazol-3-yl)pyridine

실험 절차

This compound was synthesized using the same methodology as described in Example 1 above, using 2-pyridinecarboxylic acid hydrazide, benzyl isothiocyanate and benzyl bromide as the starting materials. (M+H)+−359.

후처리

customThis compound was synthesized

출처 및 근거

ORD 기록: ord-09b5fb2419b6450987f561b77c76e85f
출처 데이터셋: uspto-grants-2009_07
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07563905B2

연결된 노트

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