Benzyl Isothiocyanate → 4-benzyl-3-[(4-chlorobenzyl)thio]-5-(2-furyl)-4H-1,2,4-triazole

HRID 229766

반응식

HRID 229766 반응식
[O:1]1[CH:5]=[CH:4][CH:3]=[C:2]1[C:6]([NH:8][NH2:9])=O.[CH2:10]([N:17]=[C:18]=[S:19])[C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1.[Cl:20][C:21]1[CH:28]=[CH:27][C:24]([CH2:25]Br)=[CH:23][CH:22]=1>>[CH2:10]([N:17]1[C:6]([C:2]2[O:1][CH:5]=[CH:4][CH:3]=2)=[N:8][N:9]=[C:18]1[S:19][CH2:25][C:24]1[CH:27]=[CH:28][C:21]([Cl:20])=[CH:22][CH:23]=1)[C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1

참가 물질

4

반응물 3

HCID 2346Benzyl IsothiocyanateHCID 187312-Furancarboxylic acid, hydrazideHCID 693291-(Bromomethyl)-4-chlorobenzene

생성물 1

HCID 71818094-benzyl-3-[(4-chlorobenzyl)thio]-5-(2-furyl)-4H-1,2,4-triazole

실험 절차

This compound was synthesized using the same methodology as described in Example 1 above, using 2-furancarboxylic acid hydrazide, benzyl isothiocyanate and 4-chlorobenzyl bromide as the starting materials. (M+H)+−382.

후처리

  1. customThis compound was synthesized

출처 및 근거

ORD 기록
ord-efda426bc2cb4df8961b54a77e95ad08
출처 데이터셋
uspto-grants-2009_07
특허 번호
US07563905B2

연결된 노트

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