p-Toluenesulfonic acid → n-(1-(1h-1,2,3-Benzotriazol-1-yl)-2,2-dimethylpropyl)-3-methylbenzamide

반응식

[C:1]1([CH3:10])[CH:6]=[CH:5][CH:4]=[C:3]([C:7]([NH2:9])=[O:8])[CH:2]=1.[CH3:11][C:12]([CH:15]=O)([CH3:14])[CH3:13].[NH:17]1[C:21]2[CH:22]=[CH:23][CH:24]=[CH:25][C:20]=2[N:19]=[N:18]1.C1(C)C=CC(S(O)(=O)=O)=CC=1>>[N:17]1([CH:15]([NH:9][C:7](=[O:8])[C:3]2[CH:4]=[CH:5][CH:6]=[C:1]([CH3:10])[CH:2]=2)[C:12]([CH3:13])([CH3:14])[CH3:11])[C:21]2[CH:22]=[CH:23][CH:24]=[CH:25][C:20]=2[N:19]=[N:18]1

참가 물질

반응물 4

HCID 6101p-Toluenesulfonic acid

HCID 12417Pivalaldehyde

HCID 69253m-Toluamide

HCID 178418385HCID 178418385, 화합물

생성물 1

HCID 18770663n-(1-(1h-1,2,3-Benzotriazol-1-yl)-2,2-dimethylpropyl)-3-methylbenzamide

실험 절차

A suspension of m-toluamide, pivaldehyde, benzotriazole, and p-toluenesulfonic acid was processed as described in Example 1C to provide the title compound.

출처 및 근거

ORD 기록: ord-455a0c55bf2248ec9c2905d9cc89d377
출처 데이터셋: uspto-grants-2002_12
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US06495576B2

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