p-Toluenesulfonic acid → HCID 18770768, 화합물

반응식

[Cl:1][C:2]1[CH:10]=[CH:9][C:5]([C:6]([NH2:8])=[O:7])=[CH:4][CH:3]=1.[Cl:11][C:12]([Cl:18])([CH2:15][CH2:16][CH3:17])[CH:13]=O.[NH:19]1[C:23]2[CH:24]=[CH:25][CH:26]=[CH:27][C:22]=2[N:21]=[N:20]1.C1(C)C=CC(S(O)(=O)=O)=CC=1>>[N:19]1([CH:13]([NH:8][C:6](=[O:7])[C:5]2[CH:9]=[CH:10][C:2]([Cl:1])=[CH:3][CH:4]=2)[C:12]([Cl:18])([Cl:11])[CH2:15][CH2:16][CH3:17])[C:23]2[CH:24]=[CH:25][CH:26]=[CH:27][C:22]=2[N:21]=[N:20]1

참가 물질

반응물 4

HCID 6101p-Toluenesulfonic acid

HCID 120844-Chlorobenzamide

HCID 27245992,2-dichloropentanal

HCID 178418385HCID 178418385, 화합물

생성물 1

HCID 18770768HCID 18770768, 화합물

실험 절차

A suspension of 4-chlorobenzamide, 2,2-dichloropentanal, benzotriazole, and p-toluenesulfonic acid was processed as in Example 1C to provide the title compound.

출처 및 근거

ORD 기록: ord-dbee098495854d07af94e0502dd05169
출처 데이터셋: uspto-grants-2002_12
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US06495576B2

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