Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzylamine → Ethyl 3-(benzylamino)butanoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzylamine | HCID 7504 | — |
| 반응물 | Ethyl trans-crotonate | HCID 429065 | — |
| 생성물 | Ethyl 3-(benzylamino)butanoate | HCID 236384 | 69% |
반응 단계
A solution of ethyl crotonate (5.0 ml, 40 mmol) and benzyl amine (4.8 ml, 44 mmol) was heated to 100° C. for 18 hs. The reaction was allowed to cool and the product was distilled at 90° C. at 200 mtorr pressure to give the ethyl 3-(benzylamino)butanoate (6.1 g, 69%) as a clear oil, MS (M+H)+=222.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06495565B2 |
| 출처 데이터셋 | uspto-grants-2002_12 |
| ORD ID | ord-848a448f0af148e48bd99e9eb0f9003f |
| 출처 메모 | uspto-grants-2002_12 |