Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
DL-alanine → 2-Methylpropyl 2-aminopropanoate hydrochloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | DL-alanine | HCID 602 | — |
| 반응물 | Isobutanol | HCID 6560 | — |
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 생성물 | 2-Methylpropyl 2-aminopropanoate hydrochloride | HCID 86200109 | — |
반응 단계
A mixture of 35.64 g (0.4 mol) of D,L-alanine (Aldrich), 44 mL (0.6 mol) of thionyl chloride (Aldrich) and 200 mL of iso-butanol was refluxed for 1.5 hours. The volatiles were removed at reduced pressure at 90° C. under reduced pressure to give the title compound as an oil, which was used without further purification.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06849650B2 |
| 출처 데이터셋 | uspto-grants-2005_02 |
| ORD ID | ord-4925e8544ee04f8dbe2b5bf9ea58b95b |
| 출처 메모 | uspto-grants-2005_02 |