4-Bromo-1,3,5-trimethylpyrazole → HCID 11280212, 화합물

HRID 230261

반응식

HRID 230261 반응식
[CH3:1][C:2]1[CH:3]=[CH:4][C:5]2[N:6]([C:8]([CH2:18][CH:19]=[O:20])=[C:9]([C:11]3[CH:16]=[CH:15][C:14]([CH3:17])=[CH:13][CH:12]=3)[N:10]=2)[CH:7]=1.Br[C:22]1[C:23]([CH3:29])=[N:24][N:25]([CH3:28])[C:26]=1[CH3:27]>>[CH3:1][C:2]1[CH:3]=[CH:4][C:5]2[N:6]([C:8]([CH2:18][C:19]([C:22]3[C:23]([CH3:29])=[N:24][N:25]([CH3:28])[C:26]=3[CH3:27])=[O:20])=[C:9]([C:11]3[CH:16]=[CH:15][C:14]([CH3:17])=[CH:13][CH:12]=3)[N:10]=2)[CH:7]=1

참가 물질

3

반응물 2

HCID 5191814-Bromo-1,3,5-trimethylpyrazoleHCID 57444052HCID 57444052, 화합물

생성물 1

HCID 11280212HCID 11280212, 화합물

실험 절차

Prepared from (6-methyl-2-p-tolyl-imidazo[1,2-a]pyridine-3-yl)-acetaldehyde 6b and 4-bromo-1,3,5-trimethyl-1H-pyrazole using the procedure of Method B described above. 1H NMR (400 MHz, CDCl3) δ 2.33 (s, 3H), 2.38 (s, 3H), 2.52 (s, 3H), 2.53 (s, 3H), 3.78 (s, 3H), 4.43 (s, 2H), 7.04 (d, J=8.8 Hz, 1H), 7.22 (m, 3H), 7.57 (m, 3H). Mass spectrum (m/e) 373 (M+).

출처 및 근거

ORD 기록
ord-e375456745c24e60a870e757def1c34a
출처 데이터셋
uspto-grants-2009_07
특허 번호
US07566725B2

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