Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Allyl Alcohol → N-(3,4dichlorophenyl)alanine Allyl Ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Allyl Alcohol | HCID 7858 | — |
| 반응물 | N-(3,4-dichlorophenyl)alanine Methyl Ester | HCID 54289412 | — |
| 생성물 | N-(3,4dichlorophenyl)alanine Allyl Ester | HCID 53861976 | — |
반응 단계
Following transesterification General Procedure AB above and using N-(3,4-dichlorophenyl)alanine methyl ester (from Example A9 above) and allyl alcohol (Aldrich), the title compound was prepared as an oil. The reaction was monitored by silica gel tlc (Rf=0.62 in 25% EtOAc/hexanes). Purification was by preparative plate chromatography (silica gel using 25% EtOAc/hexanes as the eluant).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06849650B2 |
| 출처 데이터셋 | uspto-grants-2005_02 |
| ORD ID | ord-f5c29fd86a204365875bccc1ad466609 |
| 출처 메모 | uspto-grants-2005_02 |