Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Isobutanol → N-(3,5-difluorophenyl)alanine Iso-butyl Ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Isobutanol | HCID 6560 | — |
| 반응물 | N-(3,5-difluorophenyl)alanine | HCID 53936901 | — |
| 생성물 | N-(3,5-difluorophenyl)alanine Iso-butyl Ester | HCID 54289378 | — |
반응 단계
Following General Procedure AH above and using N-(3,5-difluorophenyl)alanine (from Example AC above) and iso-butanol, the title compound was prepared as an oil. The reaction was monitored by tlc on silica gel (Rf=0.9 in 3% methanol/methylene chloride) and purification was by preparative plate chromatography (silica gel using 3% methanol/methylene chloride as the eluant).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06849650B2 |
| 출처 데이터셋 | uspto-grants-2005_02 |
| ORD ID | ord-d5613df61c1a406e8d4bc734c58fdd6b |
| 출처 메모 | uspto-grants-2005_02 |