참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Chlorotrimethylsilane | HCID 6397 | — |
| 반응물 | Linalool | HCID 6549 | — |
| 촉매 | Bismuthyl (ion) | HCID 5237718 | — |
| 생성물 | 1-Chloro-3,7-dimethyl-octa-2,6-diene | HCID 99106 | 83.2% |
반응 단계
To a mixture of 170 g linalool and 20 mg bismuth(III)-oxide heated to 60° C., 130.5 g trimethylchlorosilane were added. Then, the mixture was cooled to room temperature and the organic layer was separated. The resulting oil was purified by distillation to yield 158.35 g of a colorless oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US06437150B1 |
|---|
| 출처 데이터셋 | uspto-grants-2002_08 |
|---|
| ORD ID | ord-31741ba505834e94b3832c3054c89a99 |
|---|
| 출처 메모 | uspto-grants-2002_08 |
|---|
