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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 2304976생성일: 2026년 10월 26일

1-Dodecyl glycidyl ether → 1-O-Dodecylglycerol

https://huagongshe.com/reaction/2304976

반응식

참여 물질

역할이름HCID투입량
반응물1-Dodecyl glycidyl etherHCID 17163—
반응물Sodium BicarbonateHCID 516892—
용매WaterHCID 962—
생성물1-O-DodecylglycerolHCID 97774—

반응 조건

온도200 °C

반응 단계

In an autoclave, 249 of the resulting dodecyl glycidyl ether, 97.2 g of water and 34.8 g of sodium bicarbonate were charged and were stirred at 200° C. for 8 hours. After completion of the reaction, the reaction mixture was dehydrated at 120° C. under reduced pressure (6.67 kPa), followed by purification by distillation under reduced pressure (13 to 26 Pa, 160 to 170° C.), whereby 117 g of monododecyl glyceryl ether was obtained. As a result of gas chromatographic analysis (hereinafter abbreviated as “GLC”), it was found that the resulting product had a purity not less than 99% and the content of a chlorohydrin ether isomer different in alcohol added position and a 2-mole adduct of epichlorohydrin (hereinafter called “organochlorine compounds”, for simplicity) was not greater than 100 ppm.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US06437196B1
출처 데이터셋uspto-grants-2002_08
ORD IDord-9629739e041b4f1c80d810c998b33259
출처 메모uspto-grants-2002_08