Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethanesulfonyl chloride → N-{5-(1,4-diazepan-1-yl)-2-[(ethylsulfonyl)amino]phenyl}benzenesulfonamide hydrochloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethanesulfonyl chloride | HCID 11667 | — |
| 반응물 | N-(2-amino-5-(4-t-butyloxycarbonyl-1,4-diazepan-1-yl)-phenyl}benzenesulfonamide | HCID 22272501 | — |
| 생성물 | N-{5-(1,4-diazepan-1-yl)-2-[(ethylsulfonyl)amino]phenyl}benzenesulfonamide hydrochloride | HCID 22272439 | — |
반응 단계
N-{5-(1,4-diazepan-1-yl)-2-[(ethylsulfonyl)amino]phenyl}benzenesulfonamide hydrochloride was synthesized from N-{2-amino-5-(4-t-butyloxycarbonyl-1,4-diazepan-1-yl)-phenyl}benzenesulfonamide (0.085 g, 0.19 mmol) and ethanesulfonyl chloride (0.032 μL, 0.25 mmol) to give 29.1 mg of a light purple solid; Anal. (C24H27ClN4O3S×0.75H2O) C, H, N, S.; M+ 439.4 Calcd 439.14.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07566715B2 |
| 출처 데이터셋 | uspto-grants-2009_07 |
| ORD ID | ord-a7cb56248f08475fa37dbcab33467709 |
| 출처 메모 | uspto-grants-2009_07 |