참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Ethylene Oxide | HCID 6354 | — |
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | Dipropyleneglycol monomethyl ether | HCID 25485 | — |
| 생성물 | Dipropylene glycol monomethyl ether ethylene oxide | HCID 86583625 | — |
반응 단계
An autoclave, as equipped with a thermometer, a stirrer, and a nitrogen-introducing tube, was charged with 74 parts by weight of dipropylene glycol monomethyl ether and 1 part by weight of sodium hydroxide powder, and the internal air of the autoclave was displaced with nitrogen, and then the charged materials were heated to 130° C. Next, 426 parts by weight of ethylene oxide was introduced into the autoclave over a period of 3 hours, and then the resultant reaction mixture was aged at 130° C. for 2 hours and then cooled, thus obtaining a dipropylene glycol monomethyl ether-ethylene oxide adduct (number-average molecular weight=1,000, average molar number of addition=1.94).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 특허 번호 | US06441102B2 |
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| 출처 데이터셋 | uspto-grants-2002_08 |
|---|
| ORD ID | ord-62aef01fc3894abbacaa6bf7479c1c72 |
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| 출처 메모 | uspto-grants-2002_08 |
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