Butyl iodide → HCID 17902130, 화합물

반응식

[N+:1]([C:4]1[CH:5]=[C:6]2[C:10](=[CH:11][CH:12]=1)[N:9]=[C:8]([CH3:13])[C:7]2([CH3:15])[CH3:14])([O-:3])=[O:2].[I:16][CH2:17][CH2:18][CH2:19][CH3:20]>>[I-:16].[CH2:17]([N+:9]1[C:10]2[C:6](=[CH:5][C:4]([N+:1]([O-:3])=[O:2])=[CH:12][CH:11]=2)[C:7]([CH3:15])([CH3:14])[C:8]=1[CH3:13])[CH2:18][CH2:19][CH3:20]

참가 물질

반응물 2

HCID 10962Butyl iodide

HCID 975513H-Indole, 2,3,3-trimethyl-5-nitro-

생성물 1

HCID 17902130HCID 17902130, 화합물

실험 절차

5-Nitro-2,3,3-trimethylindole (250 mg, 1.22 mmol) and iodobutane (10 ml, 16.17 g, 87.87 mmol) were mixed and heated to reflux for 16hrs. The solvent was removed and the impure material stored at−20° C. for use in later reactions.

후처리

temperatureheated
temperatureto reflux for 16hrs
customThe solvent was removed
custom20° C.

출처 및 근거

ORD 기록: ord-0bfeec58765445f6a35d1b465bfbc39c
출처 데이터셋: uspto-grants-2004_12
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US06828116B1

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