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Propargylamine → 3-(3-(Trifluoromethyl)phenyl)-N-(2-propynyl)azetidine-1-carboxamide

HRID 2307236
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반응식

HRID 2307236 반응식
[F:1][C:2]([F:27])([F:26])C1C=C(C2CN(C(C3C=CC=CC=3)C3C=CC=CC=3)C2)C=CC=1.C(N)C#C.C([C:36]1[CH:41]=[CH:40][C:39]([CH:42]2[CH2:45][N:44]([C:46]([NH:48][CH2:49][CH:50]=[CH2:51])=[O:47])[CH2:43]2)=[CH:38][CH:37]=1)(C)(C)C>>[F:1][C:2]([F:27])([F:26])[C:41]1[CH:40]=[C:39]([CH:42]2[CH2:43][N:44]([C:46]([NH:48][CH2:49][C:50]#[CH:51])=[O:47])[CH2:45]2)[CH:38]=[CH:37][CH:36]=1
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참가 물질

4

반응물 3

HCID 239041PropargylamineHCID 226053953-(3-(Trifluoromethyl)phenyl)-1-(diphenylmethyl)azetidineHCID 226054033-(4-tert-butylphenyl)-N-(2-propenyl)azetidine-1-carboxamide

생성물 1

HCID 98172183-(3-(Trifluoromethyl)phenyl)-N-(2-propynyl)azetidine-1-carboxamide

실험 절차

This product was prepared from compound (38) and propargylamine using the procedure described for compound (12). m.p. 121° C.

출처 및 근거

ORD 기록
ord-708a03bd05a74f0e9e6a5bd0bf4064be
출처 데이터셋
uspto-grants-2004_12
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US06831078B1

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