Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-(4-Bromo-2-thienyl)-1-propanol → 4-Bromo-2-propionylthiophene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-(4-Bromo-2-thienyl)-1-propanol | HCID 22606901 | — |
| 촉매 | HCID 178418406 | HCID 178418406 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | 4-Bromo-2-propionylthiophene | HCID 818932 | — |
반응 단계
11.5 g (52 mmol) of 1-(4-bromo-2-thiophenyl)-1-propanol are dissolved in 300 mL of dichloromethane. 60 g (690 mmol) of manganese dioxide are added and the reaction medium is stirred for 14 hours and then filtered. The desired product is obtained in the form of an orange-coloured oil (m=11.4 g; Y=99%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06831106B1 |
| 출처 데이터셋 | uspto-grants-2004_12 |
| ORD ID | ord-63d3a1ebd9e74ddabe581e351eae2e72 |
| 출처 메모 | uspto-grants-2004_12 |