Ethylparaben → 4-Ethoxycarbonylphenoxy-2'-pyridylmethane

HRID 230772노트

반응식

HRID 230772 반응식
Cl.Cl[CH2:3][C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][N:5]=1.[OH:10][C:11]1[CH:16]=[CH:15][C:14]([C:17]([O:19][CH2:20][CH3:21])=[O:18])=[CH:13][CH:12]=1>>[N:5]1[CH:6]=[CH:7][CH:8]=[CH:9][C:4]=1[CH2:3][O:10][C:11]1[CH:12]=[CH:13][C:14]([C:17]([O:19][CH2:20][CH3:21])=[O:18])=[CH:15][CH:16]=1

참가 물질

3

반응물 2

HCID 8434EthylparabenHCID 23392Picolyl chloride hydrochloride

생성물 1

HCID 1911264-Ethoxycarbonylphenoxy-2'-pyridylmethane수율 83.7%

실험 절차

2-Chloromethylpyridine hydrochloride (500 mg) and ethyl 4-hydroxybenzenecarboxylate (506 mg) were processed in the same manner as in Production Example 1-1 to obtain the entitled compound (656 mg).

출처 및 근거

ORD 기록
ord-b469d348c1e04250a5471fd0753fe8d4
출처 데이터셋
uspto-grants-2009_07
특허 번호
US07566781B2

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